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how to manufacture the d enantiomer of phenylaminopropane and 34methylenedioxymethphenylaminopropane

Date Submitted: 02/01/2002 14:07:13
Category: / Law & Government / Government & Politics
Length: 40 pages (10881 words)
Re: DETAILED METHODS for NON-CHEMISTS METHamphetamine PRECURSS CLEANING/wkUP Extractomania........by Ozbee friends..........edited by Placebo INDEX: 1: Equipment 2: Ingredients 3: Method step 1: step 2: step 3: step 4: step 5: step 6: 4: Acid/Base 5: HCl-Gassing 6: Notes 1: Equipment * Various jars, glass vessels, beakers etc * PH paper, electronic PH tester * Filter paper coffeee filters * A strainer that will fit your filters nicely, so that you get better surface area then a funnel * Hair dryer, heat lamps * Hot plate, no open flames, only heat …
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…pure 2CB x HCl as a white crystaline solid. Yield - 34.0g (57%) of 2CB Hydrochloride. Purity - Single spot by TLC. NMR is clean. I have references for the two reduction steps and the bromination, but can't seem to find them. If someone asks really nicely I might be persuaded to find and post them. Also, before some jackass reads this procedure and asks me why 4 eq.of sodium borohydride is used for the reduct
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