Essay Database
how to manufacture the d enantiomer of phenylaminopropane and 34methylenedioxymethphenylaminopropane
Date Submitted: 02/01/2002 14:07:13
Category: / Law & Government / Government & Politics
Length: 40 pages (10881 words)
Category: / Law & Government / Government & Politics
Length: 40 pages (10881 words)
Re: DETAILED METHODS for NON-CHEMISTS
METHamphetamine PRECURSS CLEANING/wkUP
Extractomania........by Ozbee friends..........edited by Placebo
INDEX:
1: Equipment
2: Ingredients
3: Method
step 1:
step 2:
step 3:
step 4:
step 5:
step 6:
4: Acid/Base
5: HCl-Gassing
6: Notes
1: Equipment
* Various jars, glass vessels, beakers etc
* PH paper, electronic PH tester
* Filter paper coffeee filters
* A strainer that will fit your filters nicely,
so that you get better surface area then a funnel
* Hair dryer, heat lamps
* Hot plate, no open flames, only heat
Is this Essay helpful? Join now to read this particular paper
and access over 800,000 just like this GET BETTER GRADES
and access over 800,000 just like this GET BETTER GRADES
pure 2CB x HCl as a white crystaline solid.
Yield - 34.0g (57%) of 2CB Hydrochloride.
Purity - Single spot by TLC. NMR is clean.
I have references for the two reduction steps and the bromination, but can't seem to find them. If someone asks really nicely I might be persuaded to find and post them.
Also, before some jackass reads this procedure and asks me why 4 eq.of sodium borohydride is used for the reduct
Need a custom written paper? Let our professional writers save your time.
